Chem. Commun., 2025, Accepted Manuscript DOI: 10.1039/D5CC01976A, Communication Yanxin Liao, Huayu Wang, Shile Liu, Tianrui Liu, Lingyun Chen Herein, 1,3,5-benzenetricarboxylate (BTC) intercalation and oxygen vacancy engineering is proposed to enhance the electrochemical performance of layered double hydroxides (LDHs) nanosheets. The optimized LDH exhibits a remarkable capacity of 426...